(This was Chem 625 in previous years.) Coursework will consist of ~ 6 homework assignments (short), a written final, and 7 practical exams( 1-D proton, Cosy, 1-D carbon-13, dept on the "downstairs" AC and 1-D proton, 1-D carbon-13, and DEPT on the "upstairs" AC).
It is possible to obtain training on the NMRs without taking this class, but if at all possible, graduate students planning to use the NMR facility should take 627.
Chem 627 Schedule Fall 2009
All classes will be held in Clark 166 from 1-2:50 pm on Fridays.
Friday, 28 Aug
no class
Friday, 4 Sep
no class, cumes
Friday, 11 Sep
Class overview and NMR Theory
Friday, 18 Sep
The Theory and Practice of Data Acquisition
Instrumental parameters
Instrument Design
Locking and Shimming
Monday, 21 Sep
Start hands-on training
Friday, 25 Sep
The Theory and Practice of Data Processing
Processing Parameters
Apodizations
Data "Corrections"
Solution experiments
"Simple 1D"
Decoupling
NOE
Relaxation (T1 and T2)
APT (Attached Proton Test)
Friday, 2 Oct
No class- cumes
Friday, 9 Oct
no classs
Friday, 16 Oct
no class, UNM fall break
Friday, 23 Oct
no class
Friday, 30 Oct
Multi-dimensional experiments
COSY (Correlated Spectroscopy)
NOESY (NOE Spectroscopy)
Hetcorr/HMQC
Friday, 6 Nov
no class, cumes
Friday, 13 Nov
Introduction to Solid-State NMR
Theory
MAS/VAS/DOR
CP
CSA
2D Solids
Friday, 20 Nov
Advanced Topics
VT
Gradients
Problems, Fixes, Hints
Experiments possible on the 500 MHz NMR
"Hands-on" instrument training and testing will be scheduled
individually.
For more information, contact
Karen Ann Smith, Director NMR Facility, University of New Mexico Department of Chemistry Clark Hall Albuquerque, NM 87131-1096 karenann@unm.edu 505-277-4031 voice, 505-277-2609 fax