(This was Chem 625 in previous years.) Coursework will consist of ~ 6 homework assignments (short), a written final, and 7 practical exams( 1-D proton, Cosy, 1-D carbon-13, dept on the "downstairs" AC and 1-D proton, 1-D carbon-13, and DEPT on the "upstairs" AC).
It is possible to obtain training on the NMRs without taking this class, but if at all possible, graduate students planning to use the NMR facility should take 627.
Chem 627 Schedule Spring 2006
All classes will be held in Clark 166 from 1-2:50 pm on Fridays.
Friday, 20 Jan
no class
Friday, 27 Jan
Class overview and NMR Theory
Friday, 3 Feb
no class- cumes
Friday, 10 Feb
The Theory and Practice of Data Acquisition
Instrumental parameters
Instrument Design
Locking and Shimming
Start hands-on training
Friday, 17 Feb
The Theory and Practice of Data Processing
Processing Parameters
Apodizations
Data "Corrections"
Solution experiments
"Simple 1D"
Decoupling
NOE
Relaxation (T1 and T2)
APT (Attached Proton Test)
Friday, 24 Feb
Multi-dimensional experiments
COSY (Correlated Spectroscopy)
NOESY (NOE Spectroscopy)
Hetcorr/HMQC
Friday, 3 Mar
No class - cumes
Friday, 10 Mar
Introduction to Solid-State NMR
Theory
MAS/VAS/DOR
CP
CSA
2D Solids
Friday, 17 Mar
No class- Spring Break (UNM)
Friday, 24 Mar
Advanced Topics
VT
Gradients
Problems, Fixes, Hints
Experiments possible on the 500 MHz NMR
"Hands-on" instrument training and testing will be scheduled
individually.
For more information, contact
Karen Ann Smith, Director NMR Facility, University of New Mexico Department of Chemistry Clark Hall Albuquerque, NM 87131-1096 karenann@unm.edu 505-277-4031 voice, 505-277-2609 fax